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York Lab Technical Report — Wastewater 2025 (N5G0643) — July 23, 2025

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Technical Report

prepared for:

Village of Red Hook

7467 S Broadway Red Hook, NY 12571 Attention: J. Cavanaugh

Report Date: 07/31/2025 Client Project ID: Wastewater 2025 York Project (SDG) No.: N5G0643

CT Cert. No. PH-0800

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New York Cert. No. 11706

56 Church Hill Road #2 (203) 270-9973

Newtown, CT 06470 FAX (203) 270-3348

ClientServices@yorklab.com

www.YORKLAB.com

Page 1 of 9

Report Date: 07/31/2025 Client Project ID: Wastewater 2025 York Project (SDG) No.: N5G0643

Village of Red Hook 7467 S Broadway Red Hook, NY 12571 Attention: J. Cavanaugh

Purpose and Results

This report contains the analytical data for the sample(s) identified on the attached chain-of-custody received in our laboratory on July 23, 2025 and listed below. The project was identified as your project: Wastewater 2025 .

The analyses were conducted utilizing appropriate EPA, Standard Methods, and ASTM methods as detailed in the data summary tables.

All samples were received in proper condition meeting the customary acceptance requirements for environmental samples except those indicated under the Sample and Analysis Qualifiers section of this report.

All analyses met the method and laboratory standard operating procedure requirements except as indicated by any data flags, the meaning of which are explained in the Sample and Data Qualifiers Relating to This Work Order section of this report and case narrative if applicable.

Please contact Client Services at 203-270-9973 with any questions regarding this report.

York Sample IDClient Sample ID-Date CollectedDate Received
N5G0643-01Matrix-07/23/202507/23/2025
N5G0643-02A1 E-07/23/202507/23/2025
N5G0643-03Waste Water-07/23/202507/23/2025
N5G0643-04A2 E-07/23/202507/23/2025
N5G0643-05Waste Water-07/23/202507/23/2025
N5G0643-06A3 E-07/23/202507/23/2025
N5G0643-07Waste Water-07/23/202507/23/2025
N5G0643-08A4 E-07/23/202507/23/2025
N5G0643-09Waste Water-07/23/202507/23/2025
N5G0643-10A5 I-07/23/202507/23/2025
N5G0643-11Waste Water-07/23/202507/23/2025
-A6 I---
-Waste Water---
-A7 I---
-Waste Water---
-B1 E---
-Waste Water---
-B2 E---
-Waste Water---
-B3 E---
-Waste Water---
-B4 E---
-Waste Water---

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|||Sample Information||[TOC_2]A1 E[TOC] [TOC 1]Sample Results[TOC]|[TOC_2]A1 E[TOC] [TOC 1]Sample Results[TOC]| |---|---|---|---|---|---| |Client Sample ID:|A1 E|||York Sample ID:|N5G0643-01| |York Project (SDG)|No.|Client Project ID|Matrix|Collection Date/Time|Date Received| |N5G0643||Wastewater 2025|Waste Water|July 23, 2025 11:00 am|07/23/2025| |Field Analyses:|||Log-in/Sample Notes:|||

| Phoenix Environmental Labs, Inc. | Phoenix Environmental Labs, Inc. | Results | Analyst | | Analysis Conducted by: | Analysis Conducted by: | R | Analyzed | | [TOC_3]SM5210B-16[TOC] | [TOC_3]SM5210B-16[TOC] | MCL | Date/Time | | Units | Units | RL | Prepared | | Result | Result | - | Date/Time | | Parameter | Parameter | - | eference Method | | Qualifier | Qualifier | - | Certifications: | | - | - | - | M5210B-16 | | - | - | - | 07/23/2025 16:47 | | - | - | - | 07/23/2025 16:47 | | - | - | - | PHO | |< 4.0 Carbonaceous BOD mg/L||- S 4.00|| ||||| A2 E York Project (SDG) No. N5G0643 York Sample ID: Sample Information Client Project ID Client Sample ID: Matrix Collection Date/Time Date Received July 23, 2025 11:00 am Waste Water Wastewater 2025 [TOC_2]A2 E[TOC] 07/23/2025 N5G0643-02 Field Analyses: Log-in/Sample Notes:

| [TOC_3]Miscellaneous Physical Parameters[TOC] | - | Results | | Units | - | Analyst | | Result | - | Analyzed | | Parameter | - | Date/Time | | Qualifier | - | Prepared | | - | - | Date/Time | | - | - | Reference Method | | - | - | MCL | | - | - | RL | | - | - | SMM | | - | - | 07/25/2025 06:15 | | - | - | 07/25/2025 11:38 | | - | - | SM 2540D-2015 | | - | - | Certifications: |

--NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
--1.00
mg/L
Total Suspended Solids
2.70
A3 E
York Project (SDG) No.
N5G0643
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix
Collection Date/Time
Date Received
July 23, 2025 11:00 am
Waste Water
Wastewater 2025
[TOC_2]A3 E[TOC]
07/23/2025
N5G0643-03
Field Analyses:
Log-in/Sample Notes:

| [TOC_3]Wet Chemistry Parameters[TOC] | Results | | Units | Analyst | | Result | Analyzed | | Parameter | Date/Time | | Qualifier | Prepared | | - | Date/Time | | - | Reference Method | | - | MCL | | - | RL | | - | TCD | | - | 07/25/2025 10:09 | | - | 07/25/2025 10:09 | | - | SM 4500-NH3 D | | - | Certifications: |

-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
-0.05
-TCD
-07/24/2025 15:08
-07/25/2025 12:09
-SM 4500-N Org D
-Certifications:
-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
--
-0.40
mg/L
Ammonia Nitrogen as N
0.463
mg/L
Total Kjeldahl Nitrogen
1.66

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Newtown, CT 06470 FAX (203) 270-3348

ClientServices@yorklab.com Page 3 of 9

www.YORKLAB.com

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Sample Information[TOC_2]A4 E[TOC][TOC_2]A4 E[TOC]
Client Sample ID:A4 EYork Sample ID:N5G0643-04
York Project (SDG)No.Client Project IDMatrixCollection Date/TimeDate Received
N5G0643Wastewater 2025Waste WaterJuly 23, 2025 11:00 am07/23/2025
Field Analyses:Log-in/Sample Notes:

| Phoenix Environmental Labs, Inc. | Results | | Analysis Conducted by: | Analyst | | [TOC_3]Colilert-18[TOC] | Analyzed | | Units | Date/Time | | Result | Prepared | | Parameter | Date/Time | | Qualifier | Reference Method | | - | MCL |

-RL
-Certifications:
-Colilert-18
-07/23/2025 18:30
-07/23/2025 11:00
-PHO
-10.00
<10
Fecal Coliforms MPN
MPN/100
mls
Sample Information[TOC_2]A5 I[TOC][TOC_2]A5 I[TOC]
Client Sample ID:A5 IYork Sample ID:N5G0643-05
York Project (SDG)No.Client Project IDMatrixCollection Date/TimeDate Received
N5G0643Wastewater 2025Waste WaterJuly 23, 2025 11:00 am07/23/2025
Field Analyses:Log-in/Sample Notes:

Analysis Conducted by: Phoenix Environmental Labs, Inc.

Results

|Parameter|Result|Units|Qualifier|RL|MCL|Reference Method|Prepared Date/Time|Analyzed Date/Time|Analyst| |---|---|---|---|---|---|---|---|---|---| |Carbonaceous BOD|230|mg/L||160.00|-|SM5210B-16|07/23/2025 16:47|07/23/2025 16:47|PHO| |||||||Certifications:||||

A6 I
York Project (SDG) No.
N5G0643
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix
Collection Date/Time
Date Received
July 23, 2025 11:00 am
Waste Water
Wastewater 2025
[TOC_2]A6 I[TOC]
07/23/2025
N5G0643-06
Field Analyses:
Log-in/Sample Notes:

| [TOC_3]Miscellaneous Physical Parameters[TOC] | Results | | Units | Analyst | | Result | Analyzed | | Parameter | Date/Time | | Qualifier | Prepared | | - | Date/Time | | - | Reference Method | | - | MCL | | - | RL | | - | SMM | | - | 07/25/2025 06:15 | | - | 07/25/2025 11:38 | | - | SM 2540D-2015 | | - | Certifications: |

-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PAD
-7.14
mg/L
Total Suspended Solids
61.4

56 Church Hill Road #2 (203) 270-9973

Newtown, CT 06470 FAX (203) 270-3348

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www.YORKLAB.com

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A7 I
York Project (SDG) No.
N5G0643
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix
Collection Date/Time
Date Received
July 23, 2025 11:00 am
Waste Water
Wastewater 2025
[TOC_2]A7 I[TOC]
07/23/2025
N5G0643-07
Field Analyses:
Log-in/Sample Notes:

| [TOC_3]Wet Chemistry Parameters[TOC] | Results | | Units | Analyst | | Result | Analyzed | | Parameter | Date/Time | | Qualifier | Prepared | | - | Date/Time | | - | Reference Method | | - | MCL | | - | RL | | - | TCD | | - | 07/25/2025 10:09 | | - | 07/25/2025 10:09 | | - | SM 4500-NH3 D | | - | Certifications: |

-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
-0.10
-TCD
-07/24/2025 15:08
-07/25/2025 12:09
-SM 4500-N Org D
-Certifications:
-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
--
-0.40
mg/L
Ammonia Nitrogen as N
46.8
mg/L
Total Kjeldahl Nitrogen
52.5
Sample Information[TOC_2]B1 E[TOC][TOC_2]B1 E[TOC]
Client Sample ID:B1 EYork Sample ID:N5G0643-08
York Project (SDG)No.Client Project IDMatrixCollection Date/TimeDate Received
N5G0643Wastewater 2025Waste WaterJuly 23, 2025 11:00 am07/23/2025
Field Analyses:Log-in/Sample Notes:
Analysis Conducted by:Analysis Conducted by:PhoenixEnvironmentalLabs, Inc.
[TOC_3]SM5210B-16[TOC]Results
ParameterResultUnitsQualifierRLMCLReference MethodPrepared
Date/TimeAnalyzed
Date/TimeAnalyst
Carbonaceous BOD< 4.0mg/L4.00-SM5210B-1607/23/2025 16:4707/23/2025 16:47PHO
Certifications:
Sample Information[TOC_2]B2 E[TOC]
Client Sample ID:B2 EYork Sample ID:N5G0643-09
York Project (SDG) No.Client Project IDMatrixCollection Date/Time
Date Received
N5G0643Wastewater2025Waste WaterJuly 23, 2025 11:00 am07/23/2025
Field Analyses:Log-in/Sample Notes:
[TOC_3]Miscellaneous PhysicalParameters[TOC]Results
ParameterResultUnitsQualifierRLMCLReference MethodPrepared
Date/TimeAnalyzed
Date/TimeAnalyst
Total Suspended Solids6.00mg/L1.00-SM 2540D-201507/25/2025 06:1507/25/2025 11:38SMM
Certifications:
NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE

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Newtown, CT 06470 FAX (203) 270-3348 ClientServices@yorklab.com Page 5 of 9

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B3 E
York Project (SDG) No.
N5G0643
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix
Collection Date/Time
Date Received
July 23, 2025 11:00 am
Waste Water
Wastewater 2025
[TOC_2]B3 E[TOC]
07/23/2025
N5G0643-10
Field Analyses:
Log-in/Sample Notes:

| [TOC_3]Wet Chemistry Parameters[TOC] | Results | | Units | Analyst | | Result | Analyzed | | Parameter | Date/Time | | Qualifier | Prepared | | - | Date/Time | | - | Reference Method | | - | MCL | | - | RL | | - | TCD | | - | 07/25/2025 10:09 | | - | 07/25/2025 10:09 | | - | SM 4500-NH3 D | | - | Certifications: |

-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
-0.05
-TCD
-07/24/2025 15:08
-07/25/2025 12:09
-SM 4500-N Org D
-Certifications:
-NELAC-NY10854,CTDOH-PH-0723,NJDEP-CT005,PADE
--
-0.40
mg/L
Ammonia Nitrogen as N
0.200
mg/L
Total Kjeldahl Nitrogen
3.34
B4 E
York Project (SDG) No.
N5G0643
York Sample ID:
Sample Information
Client Project ID
Client Sample ID:
Matrix
Collection Date/Time
Date Received
July 23, 2025 11:00 am
Waste Water
Wastewater 2025
[TOC_2]B4 E[TOC]
07/23/2025
N5G0643-11
Field Analyses:
Log-in/Sample Notes:

Analysis Conducted by: Phoenix Environmental Labs, Inc.

Results

[TOC_3]Colilert-18[TOC]esults
ParameterResultUnitsQualifierRLMCLReference MethodPrepared
Date/TimeAnalyzed
Date/TimeAnalyst
Fecal Coliforms MPN<10MPN/10010.00-Colilert-1807/23/2025 11:0007/23/2025 18:30PHO
mlsCertifications:

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Definitions and Other Information

<10

<10

< 4.0 < 4.0

Analyte is not certified or the state of the samples origination does not offer certification for the Analyte.

MCL

The Maximum Contaminant Level (MCL) is the maximum concentration of a chemical that is allowed in public drinking water systems. The MCL is established by the U.S. Environmental Protection Agency (EPA). Some states have MCLs that are equal to or less than the Federally established MCL. The listed MCL value reflects the MCL established by the State where the sample was taken.

General Notes for N5G0643

  1. The RLs and MDLs (Reporting Limit and Method Detection Limit respectively) reported are adjusted for any dilution necessary due to the levels of target and/or non-target analytes and matrix interference. The RL(REPORTING LIMIT) is based upon the lowest standard utilized for the calibration where applicable.

  2. Samples are retained for a period of thirty days after submittal of report, unless other arrangements are made.

  3. York's liability for the above data is limited to the dollar value paid to York for the referenced project.

  4. This report shall not be reproduced without the written approval of York Analytical Laboratories, Inc.

  5. All analyses conducted met method or Laboratory SOP requirements. See the Sample and Data Qualifiers Section for further information.

  6. It is noted that no analyses reported herein were subcontracted to another laboratory, unless noted in the report.

  7. This report reflects results that relate only to the samples submitted on the attached chain-of-custody form(s) received by York.

Approved By:

Cassie Mosher Chemistry Director Phil Murphy Interim Microbiology Director

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Date: July 31, 2025

56 Church Hill Road #2 (203) 270-9973

Newtown, CT 06470 FAX (203) 270-3348

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References

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Recurring pattern

These other chains use the same template but are separate decisions: